Pitt Shield

Focused Ultrasound Enabled Trans-Blood Brain Barrier Delivery of Gold Nanoclusters: Effect of Surface Charges and Quantification Using Positron Emission Tomography.

Authors: Sultan D, Ye D, Heo GS, Zhang X, Luehmann H, Yue Y, Detering L, Komarov S, Taylor S, Tai YC, Rubin JB, Chen H, Liu Y

Focused ultrasound (FUS) technology is reported to enhance the delivery of <sup>64</sup> Cu-integrated ultrasmall gold nanoclusters (<sup>64</sup> Cu-AuNCs) across the blood-brain barrier (BBB) as measured by positron emission tomography (PET). To better define the optimal physical properties for brain delivery, <sup>64</sup> Cu-AuNCs with different surface charges are synthesized and characterized. In vivo biodistribution studies are performed to compare the individual organ uptake of each type of <sup>64</sup> Cu-AuNCs. Quantitative PET imaging post-FUS treatment shows site-targeted brain penetration, retention, and diffusion of the negative, neutral, and positive <sup>64</sup> Cu-AuNCs. Autoradiography is performed to compare the intrabrain distribution of these nanoclusters. PET Imaging demonstrates the effective BBB opening and successful delivery of <sup>64</sup> Cu-AuNCs into the brain. Of the three <sup>64</sup> Cu-AuNCs investigated, the neutrally charged nanostructure performs the best and is the candidate platform for future theranostic applications in neuro-oncology.

Introduction

Purpose Drug delivery with BBB opening
Study Objective To evaluate focused ultrasound–mediated trans-blood-brain barrier delivery of gold nanoclusters, investigate the effect of their surface charges on delivery, and quantify brain accumulation using positron emission tomography.
Animal model / Human subject mouse, C57BL/6, 8 weeks, male
Disease model healthy
Targeted brain region(s) Striatum
Cargo name and characteristics nanoparticle
Route of administration intravenous

Outcomes and Safety

Summary of Outcomes FUS-mediated BBB opening enabled the delivery of gold nanoclusters, with surface charge significantly influencing brain accumulation as quantified by PET.
Duration of biological effect 24 h
Safety-related matter The procedure was reported as safe with no significant tissue damage at the applied 0.3 MPa pressure.

Brain Region

Ultrasound Parameters

Ultrasound instrument single-element focused ultrasound transducer
FUS Frequency 1.0 MHz
FUS Intensity 0.3 MPa
FUS Pressure not reported
FUS Mode not reported
Pulse duration 10 ms
Duration of a single FUS session 60 s

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